Data-science-based reconstruction of 3-D membrane pore structure using a single 2-D micrograph

Conventional 2-D scanning electron microscopy (SEM) is commonly used to rapidly and qualitatively evaluate membrane pore structure. Quantitative 2-D analyses of pore sizes can be extracted from SEM, but without information about 3-D spatial arrangement and connectivity, which are crucial to the understanding of membrane pore structure. Meanwhile, experimental 3-D reconstruction via tomography is complex, expensive, and not easily accessible. Here, we employ data science tools to demonstrate a proof-of-principle reconstruction of the 3-D structure of a membrane using a single 2-D image pulled from a 3-D tomographic data set. The reconstructed and experimental 3-D structures were then directly compared, with important properties such as mean pore radius, mean throat radius, coordination number and tortuosity differing by less than 15%. The developed algorithm could dramatically improve the ability of the membrane community to characterize membranes, accelerating the design and synthesis of membranes with desired structural and transport properties.

© This manuscript version is made available under the CC-BY-NC-ND 4.0 license https://creativecommons.org/licenses/by-nc-nd/4.0/

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Work Title Data-science-based reconstruction of 3-D membrane pore structure using a single 2-D micrograph
Access
Open Access
Creators
  1. Hooman Chamani
  2. Arash Rabbani
  3. Kaitlyn P. Russell
  4. Andrew L. Zydney
  5. Enrique D. Gomez
  6. Jason Hattrick-Simpers
  7. Jay R. Werber
Keyword
  1. Data science
  2. 3-D reconstruction
  3. Membrane microstructure
  4. Electron microscopy
  5. Pore analysis
License CC BY-NC-ND 4.0 (Attribution-NonCommercial-NoDerivatives)
Work Type Article
Publisher
  1. Journal of Membrane Science
Publication Date April 24, 2023
Publisher Identifier (DOI)
  1. https://doi.org/10.1016/j.memsci.2023.121673
Deposited July 24, 2023

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Version 1
published

  • Created
  • Added Manuscript.docx
  • Added Creator Hooman Chamani
  • Added Creator Arash Rabbani
  • Added Creator Kaitlyn P. Russell
  • Added Creator Andrew L. Zydney
  • Added Creator Enrique D. Gomez
  • Added Creator Jason Hattrick-Simpers
  • Added Creator Jay R. Werber
  • Published
  • Updated Keyword, Publication Date Show Changes
    Keyword
    • Data science, 3-D reconstruction, Membrane microstructure, Electron microscopy, Pore analysis
    Publication Date
    • 2023-07-15
    • 2023-04-24
  • Updated